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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide

6-(3-(HYDROXYMETHYL)PHENYL)NAPHTHALEN-2-OL synthesis

1synthesis methods
15231-91-1 Synthesis
6-Bromo-2-naphthol

15231-91-1
391 suppliers
$7.00/5g

3-(Hydroxymethyl)phenylboronic acid

87199-15-3
292 suppliers
$8.00/5g

6-(3-(HYDROXYMETHYL)PHENYL)NAPHTHALEN-2-OL

1017858-90-0
4 suppliers
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Yield:1017858-90-0 49%

Reaction Conditions:

with potassium carbonate;palladium diacetate in 1,2-dimethoxyethane;ethanol;water at 150; for 0.0833333 h;microwave irradiation;Suzuki coupling;

References:

Frotscher, Martin;Ziegler, Erika;Marchais-Oberwinkler, Sandrine;Kruchten, Patricia;Neugebauer, Alexander;Fetzer, Ludivine;Scherer, Christiane;Müller-Vieira, Ursula;Messinger, Josef;Thole, Hubert;Hartmann, Rolf W. [Journal of Medicinal Chemistry,2008,vol. 51,# 7,p. 2158 - 2169]