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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide

6,7-dihydro-3-methyl-5H-1-pyrindine synthesis

1synthesis methods
2-Methylpropenaloxime

28051-68-5
1 suppliers
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Cyclopentanone

120-92-3
399 suppliers
$11.00/25g

6,7-dihydro-3-methyl-5H-1-pyrindine

28712-61-0
11 suppliers
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1,2,3,5,6,7-hexahydrodicyclopenta[b,e]pyridine

34421-99-3
7 suppliers
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-

Yield:28712-61-0 17% ，34421-99-3 18%

Reaction Conditions:

with piperidine hydrochloride in toluene at 200; for 2 h;autoclave;

References:

Vijn;Arts;Green;Castelijns [Synthesis,1994,# 6,p. 573 - 578]