6-Amino-3-methyl-1,3-benzoxazol-2(3H)-one, 90% synthesis
- Product Name:6-Amino-3-methyl-1,3-benzoxazol-2(3H)-one, 90%
- CAS Number:99584-10-8
- Molecular formula:C8H8N2O2
- Molecular Weight:164.16
101084-61-1
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99584-10-8
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Yield:99584-10-8 96%
Reaction Conditions:
Stage #1: 3-methyl-6-nitro-2(3H)-benzoxazolonewith hydrogenchloride;tin(ll) chloride in ethanol;water; for 1.5 h;Reflux;
Stage #2: with sodium hydroxide in ethanol;water;
References:
Guelkok, Yildiz;Bicer, Tuba;Onurdag, Fatma Kaynak;Oezgen, Selda;Sahin, Mustafa Fethi;Dogruer, Deniz Songuel [Turkish Journal of Chemistry,2012,vol. 36,# 2,p. 279 - 291] Location in patent:experimental part
4694-91-1
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99584-10-8
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21892-80-8
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99584-10-8
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121-88-0
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99584-10-8
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59-49-4
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$6.00/5g
99584-10-8
28 suppliers
$45.00/50mg