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6-Benzothiazolamine, 2-chloro-N,N-dimethyl- synthesis

1synthesis methods
-

Yield:1055343-40-2 43%

Reaction Conditions:

with sodium tris(acetoxy)borohydride in 1,1-dichloroethane;water at 20; for 1 h;

References:

Reddy, Gadarla Randheer;Thompson, Walter C.;Miller, Stephen C. [Journal of the American Chemical Society,2010,vol. 132,# 39,p. 13586 - 13587] Location in patent:supporting information; experimental part