6-BROMO-1,3-DIHYDRO-INDOLE-2-THIONE synthesis
- Product Name:6-BROMO-1,3-DIHYDRO-INDOLE-2-THIONE
- CAS Number:848649-94-5
- Molecular formula:C8H6BrNS
- Molecular Weight:228.11
99365-40-9
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Yield:848649-94-5 84%
Reaction Conditions:
Stage #1: 6-bromo-2,3-dihydro-1H-indole-2-onewith sodium hydrogencarbonate in tetrahydrofuran at 20;Inert atmosphere;Schlenk technique;
Stage #2: with tetraphosphorus decasulfide in tetrahydrofuran at 20;Inert atmosphere;Schlenk technique;
References:
Gopal, Braj;Singh, Prasoon Raj;Kumar, Madan;Goswami, Avijit [Journal of Organic Chemistry,2023,vol. 88,# 1,p. 132 - 142] Location in patent:supporting information
3460-18-2
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100487-81-8
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