Welcome to chemicalbook!
Chinese English Japanese Germany Korea
400-158-6606
logo
Inquriy
Try our best to find the right business for you.
Messages
Do not miss inquiry messages Please log in to view all inquiry messages.
My chemicalbook

Welcome back!

Structured search
18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List 6-BROMO-2(1H)-QUINOLONE
1810-66-8

6-BROMO-2(1H)-QUINOLONE synthesis

13synthesis methods
(2E)-N-(4-Bromophenyl)-3-ethoxy-2-propenamide

327058-51-5
32 suppliers
$150.00/250 mg

6-BROMO-2(1H)-QUINOLONE

1810-66-8
179 suppliers
$10.00/250mg

-

Yield: 97%

Reaction Conditions:

with sulfuric acid at 100;

Steps:

6.b
6-Bromo-2(1 /-/)-quinolinone. The solution of the compound from Example 6 a) (6.0 g, 22.2 mmol) in concentrated H2SO4 (30 mL) was heated in 100 0C EPO overnight. The mixture was cooled to ambient temperature and quenched with ice water. The precipitate was filtered, washed with water and dried in vacuo to afford the title compound as a white solid (4.8 g, 97%). MS(ES+) m/e 225 [M+H]+.

References:

SMITHKLINE BEECHAM CORPORATION WO2006/132739, 2006, A2 Location in patent:Page/Page column 35-36

106-40-1 Synthesis
4-Bromoaniline

106-40-1
476 suppliers
$12.00/5g

6-BROMO-2(1H)-QUINOLONE

1810-66-8
179 suppliers
$10.00/250mg

References
N-(4-bromophenyl)cinnamamide

54934-81-5
22 suppliers
inquiry

6-BROMO-2(1H)-QUINOLONE

1810-66-8
179 suppliers
$10.00/250mg

References
Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
0 suppliers
inquiry

6-BROMO-2(1H)-QUINOLONE

1810-66-8
179 suppliers
$10.00/250mg

References
Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
0 suppliers
inquiry

6-BROMO-2(1H)-QUINOLONE

1810-66-8
179 suppliers
$10.00/250mg

References

6-BROMO-2(1H)-QUINOLONE Related Search:

6-Bromoquinoxaline 6-bromoquinoxalin-2(1H)-one 6-BROMO-QUINAZOLIN-4-YLAMINE 6-BROMOQUINOLINE-3-CARBOXYLIC ACID 6-Bromoquinazoline 6-BroMoquinoline-2-carbaldehyde 6-BROMO-2-HYDROXYQUINOLINE-4-CARBOXYLIC ACID 6-bromo-3-methyl-3H-dibenz[f,ij]isoquinoline-2,7-dione 6-BROMO-4-METHYLQUINOLIN-2(1H)-ONE 6-Bromoquinoline