(6-BroMobenzo[b]thiophen-2-yl)Methanol synthesis

8synthesis methods

Product Name:(6-BroMobenzo[b]thiophen-2-yl)Methanol
CAS Number:374933-76-3
Molecular formula:C9H7BrOS
Molecular Weight:243.12

105191-64-8 Synthesis

Ethyl 6-broMo-1-benzothiophene-2-carboxylate

105191-64-8
52 suppliers
$55.00/250mg

374933-76-3
40 suppliers
$69.00/250mg

Yield:374933-76-3 96%

Reaction Conditions:

with lithium borohydride in tetrahydrofuran at 60; for 3 h;

Steps:

3 3. Preparation of (6-bromo-benzo[b]thiophen-2-yl)-methanol

(a) tetrahydrofuran, LiBH₄, 60° C., 3 h [0308] The substance was obtained according to the general procedure, yielding the title compound as a white solid (96%)

References:

US2014/303207,2014,A1 Location in patent:Paragraph 0307; 0308

6-BROMO-BENZO[B]THIOPHENE-2-CARBOXY LIC ACID METHYL ESTER

360576-01-8
89 suppliers
$9.00/100mg

374933-76-3
40 suppliers
$69.00/250mg

References

57848-46-1
384 suppliers
$9.00/1g

374933-76-3
40 suppliers
$69.00/250mg

References

2365-48-2 Synthesis

2365-48-2
341 suppliers
$14.00/25g

57848-46-1
384 suppliers
$9.00/1g

374933-76-3
40 suppliers
$69.00/250mg

References

5629-98-1 Synthesis

N-(4-dimethylaminophenyl)-2-(5-methyl-2-propan-2-yl-phenoxy)acetamide

5629-98-1
89 suppliers
$8.00/250mg

374933-76-3
40 suppliers
$69.00/250mg

References