6-(BROMOMETHYL)-4-CHLOROTHIENO[2,3-D]PYRIMIDINE synthesis

3synthesis methods

Product Name:6-(BROMOMETHYL)-4-CHLOROTHIENO[2,3-D]PYRIMIDINE
CAS Number:108099-55-4
Molecular formula:C7H4BrClN2S
Molecular Weight:0

2-AMINO-5-METHYL-THIOPHENE-3-CARBOXYLIC ACID ETHYL ESTER

4815-32-1
107 suppliers
$12.00/1mg

6-(BROMOMETHYL)-4-CHLOROTHIENO[2,3-D]PYRIMIDINE

108099-55-4
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: 73 percent / 2 h / Heating
2: 82 percent / phosphorus oxychloride, DMF / 1,2-dichloro-ethane / 1.5 h / Heating
3: 55 percent / N-bromosuccinimide, benzoylperoxide / CCl₄ / 1.5 h / Heating

References:

Kaplina, N. V.;Grinev, A. N.;Bogdanova, G. A.;Alekseeva, L. M.;Pushkina, T. V.;et al. [Pharmaceutical Chemistry Journal,1987,vol. 21,# 2,p. 126 - 129][Khimiko-Farmatsevticheskii Zhurnal,1987,vol. 21,# 2,p. 197 - 200]

4-CHLORO-6-METHYLTHIENO[2,3-D]PYRIMIDINE

106691-21-8
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$45.00/50mg

108099-55-4
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References

$BUTTPARK 146\18-29$

108831-66-9
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$30.00/20mg

108099-55-4
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References