6-Chlorohex-1-ene synthesis
- Product Name:6-Chlorohex-1-ene
- CAS Number:928-89-2
- Molecular formula:C6H11Cl
- Molecular Weight:118.6
105-53-3
736 suppliers
$5.00/25g
928-89-2
113 suppliers
$10.00/1g
Yield: 81%
Reaction Conditions:
with sodium in ethanol
Steps:
S.2.2 2)
To 1000 ml of absolute ethanol was added 4 g (0.174 mole) of sodium, and 20 g (0.125 mole) of diethyl malonate was then added thereto. Further, 14 g (0.118 mole) of 5-hexenyl chloride as obtained in (1) above was slowly added thereto, followed by refluxing for 2 hours. The reaction mixture was freed of the solvent by distillation, and the residue was distilled to obtain 23.2 g (yield: 81%) of diethyl 5-hexenylmalonate having a boiling point of 115°-116° C./3 mmHg.
References:
Takasago International Corporation US5141921, 1992, A
10297-06-0
92 suppliers
$22.00/1 g
928-89-2
113 suppliers
$10.00/1g
18922-06-0
0 suppliers
inquiry
928-89-2
113 suppliers
$10.00/1g
2622-05-1
151 suppliers
$40.00/500mg
109-70-6
477 suppliers
$10.00/5g
928-89-2
113 suppliers
$10.00/1g
10297-06-0
92 suppliers
$22.00/1 g
544-10-5
232 suppliers
$13.00/5g
928-89-2
113 suppliers
$10.00/1g