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ChemicalBook CAS DataBase List 6-Chlorohexyl methacrylate

6-Chlorohexyl methacrylate synthesis

3synthesis methods
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Yield: 91.6%

Reaction Conditions:

with zinc(II) chloride in cyclohexane at 80; for 6 h;

Steps:

1
To a 2000 ml four-necked round bottom flask equipped with a mechanical stirrer,a thermometer and a reflux condenser, 408 g of 1,6-epoxyhexane, Nitroxide free piperidine alcohol polymerization inhibitor 1.3g, 100 g of cyclohexane, 7.5 g of zinc chloride, and the mixture was heated to 80 ° C with stirring Add 209g methacryloyl chloride, reflux reaction 6h. The results of gas chromatography showed that the raw material methacryloyl chloride completely reacted, The yield of 6-chlorohexyl methacrylate was 91.6%.

References:

China National Offshore Oil Corporation;CNOOC Tianjin Chemical Research & Design Institute Co.;CNOOC Energy Technology & Services Limited;Song, Xiao Li;Zhou, Li Shan;you, na;Teng, Hou Kai CN105541618, 2016, A Location in patent:Paragraph 0014-0015

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