6-ETHOXY-BENZO[1,3]DIOXOLE-5-CARBALDEHYDE synthesis

1synthesis methods

Product Name:6-ETHOXY-BENZO[1,3]DIOXOLE-5-CARBALDEHYDE
CAS Number:75889-50-8
Molecular formula:C10H10O4
Molecular Weight:194.18

87590-41-8
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6-ETHOXY-BENZO[1,3]DIOXOLE-5-CARBALDEHYDE

75889-50-8
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$188.00/500mg

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 41 percent / Br₂ / CCl₄ / 2 h / 0 °C
2: 1.) 1.6 M n-BuLi in hexanes / 1.) ether, -78 deg C, 10 min, 2.) from -78 deg C to RT, 30 min

References:

Getahun, Zelleka;Jurd, Leonard;Chu, Ping S.;Lin, Chii M.;Hamel, Ernest [Journal of Medicinal Chemistry,1992,vol. 35,# 6,p. 1058 - 1067]