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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide

6-Fluorobenzo[b]thiophen-3-amine synthesis

3synthesis methods
3939-09-1 Synthesis
2,4-Difluorobenzonitrile

3939-09-1
294 suppliers
$10.00/5g

6-Fluorobenzo[b]thiophen-3-amine

142364-00-9
3 suppliers
inquiry

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Yield:-

Steps:

Multi-step reaction with 2 steps
1: 8.65 g / LiOH*H2O / dimethylformamide / -10 °C
2: 1-methylpiperazine / various solvent(s) / 2 h / 176 °C

References:

Hrib, Nicholas J.;Jurcak, John G.;Bregna, Deborah E.;Burgher, Kendra L.;Hartman, Harold B.;Kafka, Sharon;Kerman, Lisa L.;Kongsamut, Sam;Roehr, Joachim E.;Szewczak, Mark R.;Woods-Kettelberger, Ann T.;Corbett, Roy [Journal of Medicinal Chemistry,1996,vol. 39,# 20,p. 4044 - 4057]

3-AMINO-6-FLUORO-BENZO[B]THIOPHENE-2-CARBOXYLIC ACID METHYL ESTER

142363-99-3
16 suppliers
inquiry

6-Fluorobenzo[b]thiophen-3-amine

142364-00-9
3 suppliers
inquiry

References
109-01-3 Synthesis
1-Methylpiperazine

109-01-3
651 suppliers
$5.00/5G

872-50-4 Synthesis
N-Methyl-2-pyrrolidone

872-50-4
887 suppliers
$10.00/100ML

3-AMINO-6-FLUORO-BENZO[B]THIOPHENE-2-CARBOXYLIC ACID METHYL ESTER

142363-99-3
16 suppliers
inquiry

6-Fluorobenzo[b]thiophen-3-amine

142364-00-9
3 suppliers
inquiry

References