ChemicalBook CAS DataBase List 6-Hydroxysugiol

6-Hydroxysugiol synthesis

5synthesis methods

Product Name:6-Hydroxysugiol
CAS Number:55898-07-2
Molecular formula:C20H28O3
Molecular Weight:316.43

Phenanthrene, 1,2,3,4,4a,10a-hexahydro-6-methoxy-1,1,4a-trimethyl-7-(1-methylethyl)-, (4aS,10aS)-

70614-86-7
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55898-07-2
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Yield:55898-07-2 70%

Reaction Conditions:

Stage #1: (4aS,10aS)-7-isopropyl-6-methoxy-1,1,4a-trimethyl-1,2,3,4,4a,10a-hexahydrophenanthrenewith 3,3-dimethyldioxirane in dichloromethane;acetone at 25; for 0.333333 h;
Stage #2: with sodium thioethylate in dichloromethane;N,N-dimethyl-formamide;acetone at 90; for 8 h;

References:

Córdova-Guerrero;Andrés, Lucía San;Leal-Orozco, Alma E.;Padrón, José M.;Cornejo-Bravo;León, Francisco [Tetrahedron Letters,2013,vol. 54,# 33,p. 4479 - 4482]

1,1,4a-trimethyl-7-propan-2-yl-2,3,4,9,10,10a-hexahydrophenanthrene

19407-28-4
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55898-07-2
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References

15340-79-1
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55898-07-2
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References

3-Phenanthrenol, 4b,5,6,7,8,8a,9,10-octahydro-4b,8,8-trimethyl-2-(1-methylethyl)-, (4bS,8aS)-

514-62-5
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55898-07-2
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References

9(1H)-Phenanthrenone, 2,3,4,4a,10,10a-hexahydro-6-methoxy-1,1,4a-trimethyl-7-(1-methylethyl)-, (4aS,10aS)-

901-41-7
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55898-07-2
15 suppliers
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References