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ChemicalBook CAS DataBase List 6-IODO-3 H-ISOBENZOFURAN-1-ONE

6-IODO-3 H-ISOBENZOFURAN-1-ONE synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: KNO3; H2SO4
2.1: Fe / acetic acid; ethyl acetate; H2O / 1 h / Heating
2.2: 86 percent / NaHCO3 / 0.17 h / Heating
3.1: HNO2; HCl
3.2: KI; CuI

References:

Abaev, Vladimir T.;Dmitriev, Artem S.;Gutnov, Andrey V.;Podelyakin, Sergey A.;Butin, Alexander V. [Journal of Heterocyclic Chemistry,2006,vol. 43,# 5,p. 1195 - 1204]

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