![](/CAS/GIF/1078-19-9.gif)
6-methoxy-1-tetralone synthesis
- Product Name:6-methoxy-1-tetralone
- CAS Number:1078-19-9
- Molecular formula:C11H12O2
- Molecular Weight:176.21
![1078-19-9.png 1078-19-9.png](/NewsImg/2022-11-22/6380472076727661623074941.jpg)
![6-METHOXY-1,2,3,4-TETRAHYDRONAPHTHALEN-1-OL](/StructureFile/ChemBookStructure9/GIF/CB2193298.gif)
16821-32-2
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![6-methoxy-1-tetralone](/CAS/GIF/1078-19-9.gif)
1078-19-9
363 suppliers
$6.00/5g
Yield:1078-19-9 95%
Reaction Conditions:
with 1-hydroxy-1H-1,2,3-benziodoxathiole 1,3,3-trioxide;Oxone;cetyltrimethylammonim bromide in water at 20; for 2 h;Green chemistry;chemoselective reaction;
Steps:
IBS-catalysed alcohol oxidation in CTAB micelle; general procedure
General procedure: The alcohol (2 mmol) was added to a solution of IBS (0.02 mmol, 0.01 eq), oxone (2.2 mmol, 1.1 equiv.) and 3 wt% CTAB solution (5 mL). The mixture was stirred at room temperature. The reaction was monitored by TLC. After completion, the solution was extracted with CH2Cl2 (3 × 10 mL). The combined organic phase was then filtered through a pad of silica gel and evaporated under vacuum to afford the desired product.
References:
Liu, Yangyang;Wang, Boliang [Journal of Chemical Research,2014,vol. 38,# 7,p. 427 - 431]
![6-METHOXY-1,2,3,4-TETRAHYDRONAPHTHALENE](/CAS/GIF/1730-48-9.gif)
1730-48-9
64 suppliers
$46.00/5mL
![6-methoxy-1-tetralone](/CAS/GIF/1078-19-9.gif)
1078-19-9
363 suppliers
$6.00/5g
![Benzenebutanoic acid, 3-methoxy-, methyl ester](/CAS/20210111/GIF/57816-04-3.gif)
57816-04-3
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![6-methoxy-1-tetralone](/CAS/GIF/1078-19-9.gif)
1078-19-9
363 suppliers
$6.00/5g
![2-PHENOXYBENZONITRILE](/CAS/GIF/6476-32-0.gif)
6476-32-0
45 suppliers
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![6-methoxy-1-tetralone](/CAS/GIF/1078-19-9.gif)
1078-19-9
363 suppliers
$6.00/5g
![6-METHOXY-1,2,3,4-TETRAHYDRONAPHTHALENE](/CAS/GIF/1730-48-9.gif)
1730-48-9
64 suppliers
$46.00/5mL
![7-Methoxy-1-tetralone](/CAS/GIF/6836-19-7.gif)
6836-19-7
489 suppliers
$14.00/5g
![6-methoxy-1-tetralone](/CAS/GIF/1078-19-9.gif)
1078-19-9
363 suppliers
$6.00/5g