6-Methoxy-N,N-dimethyl-2-pyrazinamine synthesis
- Product Name:6-Methoxy-N,N-dimethyl-2-pyrazinamine
- CAS Number:136309-09-6
- Molecular formula:C7H11N3O
- Molecular Weight:153.18
67-56-1
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Yield:136309-09-6 97%
Reaction Conditions:
with t-BuBrettPhos;[(2-di-tert-butylphosphino-3,6-dimethoxy-2’,4’,6’-triisopropyl-1,1’-biphenyl)-2-(2’-amino-1,1‘-biphenyl)]palladium(II) methanesulfonate;sodium t-butanolate in 1,4-dioxane at 20; for 20 h;Sealed tube;Inert atmosphere;
References:
Cheung, Chi Wai;Buchwald, Stephen L. [Organic Letters,2013,vol. 15,# 15,p. 3998 - 4001] Location in patent:supporting information