ChemicalBook CAS DataBase List 6-methyl-1,2,4-benzenetriol

6-methyl-1,2,4-benzenetriol synthesis

10synthesis methods

Product Name:6-methyl-1,2,4-benzenetriol
CAS Number:767-81-7
Molecular formula:C7H8O3
Molecular Weight:140.14

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Yield:-

Steps:

Multi-step reaction with 5 steps
1: 98 percent / H₂, AcOH / 10percent Pd/C / ethyl acetate / 72 h
2: 70 percent / aq. KH₂PO₄, (KSO₃)2NO / diethyl ether / 1 h
3: 98 percent / aq. TiCl₃ / acetone / 0.17 h / Ambient temperature
4: 28 percent / K₂CO₃ / acetone / 12 h / Heating
5: 66 percent / BBr₃ / CH₂Cl₂ / 12 h / 25 °C

References:

Singh, Udai S.;Scannell, Ralph T.;An, Haoyun;Carter, Barbara J.;Hecht, Sidney M. [Journal of the American Chemical Society,1995,vol. 117,# 51,p. 12691 - 12699]

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References

28814-66-6
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References

611-68-7
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References

Benzene, 1-methyl-3,5-bis(phenylmethoxy)-

36776-43-9
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References

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