6-METHYL-BENZO[1,3]DIOXOLE-5-CARBALDEHYDE synthesis
- Product Name:6-METHYL-BENZO[1,3]DIOXOLE-5-CARBALDEHYDE
- CAS Number:58343-54-7
- Molecular formula:C9H8O3
- Molecular Weight:164.16
7145-99-5
88 suppliers
$60.00/500mg
4885-02-3
190 suppliers
$10.00/1g
58343-54-7
27 suppliers
$45.00/50mg
Yield:58343-54-7 96%
Reaction Conditions:
Stage #1: 5-methyl-1,3-benzodioxole;Dichloromethyl methyl ether in dichloromethane at 0;
Stage #2: with titanium tetrachloride in dichloromethane at 20;
References:
Aslam, Shazia N.;Stevenson, Philip C.;Phythian, Sara J.;Veitch, Nigel C.;Hall, David R. [Tetrahedron,2006,vol. 62,# 17,p. 4214 - 4226]
7145-99-5
88 suppliers
$60.00/500mg
58343-54-7
27 suppliers
$45.00/50mg