6-METHYLPYRIDINE-2-BORONIC ACID PINACOL ESTER synthesis
- Product Name:6-METHYLPYRIDINE-2-BORONIC ACID PINACOL ESTER
- CAS Number:1096689-44-9
- Molecular formula:C12H18BNO2
- Molecular Weight:219.09
109-06-8
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Yield:1096689-44-9 1%
Reaction Conditions:
with catalyst: [Ir(COD)Cl]2/2bpy in further solvent(s);under Ar; (C5H4N)CH3 (60 mmol) added to pinacolborane (2 mmol) and 1.5 mol % (Ir(COD)Cl)2 and 1.5 mol% bpy; stirred (80°C, 6 h); solvent removed (vac., room temp.); residue chromd. (silica gel, CH2Cl2);
References:
Mertins, Kristin;Zapf, Alexander;Beller, Matthias [Journal of Molecular Catalysis A: Chemical,2004,vol. 207,# 1,p. 21 - 25]