ChemicalBook CAS DataBase List 5-Chloro-6-Methoxy-α-Methyl-2-naphthaleneacetic Acid

5-Chloro-6-Methoxy-α-Methyl-2-naphthaleneacetic Acid synthesis

5synthesis methods

Product Name:5-Chloro-6-Methoxy-α-Methyl-2-naphthaleneacetic Acid
CAS Number:60424-17-1
Molecular formula:C14H13ClO3
Molecular Weight:264.7

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5-Chloro-6-Methoxy-α-Methyl-2-naphthaleneacetic Acid

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Yield:-

Steps:

Multi-step reaction with 5 steps
1: 63 percent / Mg / tetrahydrofuran / 4 h / -40 °C
2: 10 percent / propylene oxide / H₂O; acetone / Irradiation; pH neutral
3: 85 percent / SO₂Cl₂ / CCl₄ / 12 h / 50 °C
4: propylene oxide / methanol / Irradiation; pH neutral
5: OH(-)

References:

Sonawane, Harikisan;Bellur, Nanjundiah S.;Kulkarni, Dilip G.;Ayyangar, Nagaraj R. [Tetrahedron,1994,vol. 50,# 4,p. 1243 - 1260]