1,3,2-Dioxathiolane, 4-[(phenylmethoxy)methyl]-5-(trifluoromethyl)-, 2,2-dioxide, (4S,5R)- synthesis

3synthesis methods

Product Name:1,3,2-Dioxathiolane, 4-[(phenylmethoxy)methyl]-5-(trifluoromethyl)-, 2,2-dioxide, (4S,5R)-
CAS Number:610272-50-9
Molecular formula:C11H11F3O5S
Molecular Weight:312.26

Benzene, [[[(2E)-4,4,4-trifluoro-2-buten-1-yl]oxy]methyl]-

610272-47-4
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1,3,2-Dioxathiolane, 4-[(phenylmethoxy)methyl]-5-(trifluoromethyl)-, 2,2-dioxide, (4S,5R)-

610272-50-9
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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: 96 percent / (DHQD)PHAL; OsO₄; K₂CO₃ / K₃Fe(CN)6; MeSO₂NH₄ / 2-methyl-propan-2-ol; H₂O / 48 h / 20 °C
2.1: SOCl₂; Et₃N
2.2: NaIO₄; RuCl₃

References:

Jiang, Zhong-Xing;Qing, Feng-Ling [Journal of Organic Chemistry,2004,vol. 69,# 16,p. 5486 - 5489]

2,3-Butanediol, 1,1,1-trifluoro-4-(phenylmethoxy)-, (2R,3S)-

610272-49-6
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610272-50-9
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Benzene, [[[(2E)-3-bromo-2-propen-1-yl]oxy]methyl]-

610272-48-5
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610272-50-9
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References