(3aR,4R,5R,6aS)-5-[[(1,1-DiMethylethyl)diMethylsilyl]oxy]-4-[(1E,3S)-3-[[(1,1-diMethylethyl)diMethylsilyl]oxy]-1-octen-1-yl]hexahydro-2H-cyclopenta[b]furan-2-one synthesis

11synthesis methods

Product Name:(3aR,4R,5R,6aS)-5-[[(1,1-DiMethylethyl)diMethylsilyl]oxy]-4-[(1E,3S)-3-[[(1,1-diMethylethyl)diMethylsilyl]oxy]-1-octen-1-yl]hexahydro-2H-cyclopenta[b]furan-2-one
CAS Number:61628-05-5
Molecular formula:C27H52O4Si2
Molecular Weight:496.87

75-77-4
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(3aR,4R,5R,6aS)-5-((tert-butyldimethylsilyl)oxy)-4-((S,E)-3-hydroxyoct-1-en-1-yl)hexahydro-2H-cyclopenta[b]furan-2-one

64072-30-6
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(3aR,4R,5R,6aS)-5-[[(1,1-DiMethylethyl)diMethylsilyl]oxy]-4-[(1E,3S)-3-[[(1,1-diMethylethyl)diMethylsilyl]oxy]-1-octen-1-yl]hexahydro-2H-cyclopenta[b]furan-2-one

61628-05-5
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Yield:61628-05-5 98%

Reaction Conditions:

with 1H-imidazole in dichloromethane at 20; for 12 h;

References:

Zanoni, Giuseppe;D'Alfonso, Alessandro;Porta, Alessio;Feliciani, Lazzaro;Nolan, Steven P.;Vidari, Giovanni [Tetrahedron,2010,vol. 66,# 38,p. 7472 - 7478] Location in patent:experimental part

18162-48-6 Synthesis