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62054-77-7

methyl 3-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-yl)propanoate synthesis

1synthesis methods
2033-24-1 Synthesis
2,2-Dimethyl-1,3-dioxane-4,6-dione

2033-24-1
648 suppliers
$6.00/25g

acrylic acid methyl ester

292638-85-8
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Yield:62054-77-7 92%

Reaction Conditions:

with N-benzyl-trimethylammonium hydroxide;potassium carbonate in acetonitrile at 50 - 60; for 8 h;Michael addition;

References:

Chande, Madhukar S.;Khanwelkar, Rahul R. [Tetrahedron Letters,2005,vol. 46,# 45,p. 7787 - 7792]