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1-(5-AMINO-2-PHENYL-[1,3,4]THIADIAZOL-3-YL)-ETHANONE synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 56 percent / pyridine; acetone / 1.) 0 deg C, 2.) RT, 2 h
2: 77 percent / Hydrazine hydrate (85percent) / 3 h / Ambient temperature

References:

Kubota, Seiju;Ueda, Yasufumi;Fujikane, Kazuichi;Toyooka, Kouhei;Shibuya, Masayuki [Journal of Organic Chemistry,1980,vol. 45,# 8,p. 1473 - 1477]

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