tert-Butyl(2-hydrazinyl-2- oxoethyl)(Methyl)carbaMate synthesis
- Product Name:tert-Butyl(2-hydrazinyl-2- oxoethyl)(Methyl)carbaMate
- CAS Number:633328-19-5
- Molecular formula:C8H17N3O3
- Molecular Weight:203.24
145060-76-0
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Yield:633328-19-5 86%
Reaction Conditions:
with hydrazine hydrate in ethanol at 20; for 4 h;
Steps:
1
Compound B1 (500 mg, 2.30 mmol) was dissolved in ethanol (10 mL), and hydrazine hydrate (2 mL) was added with stirring. Then the stirring was continued at room temperature, monitored by TLC plate, and the reaction was completed in 4 h. The reaction system was concentrated and purified by column chromatography (DCM:MeOH=20:1) to obtain compound B2 (400 mg, yield: 86%).
References:
CN113121521,2021,A Location in patent:Paragraph 0010; 0018
24424-99-5
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