ChemicalBook CAS DataBase List 2-[6-(acetylphenylamino)hexa-1,3,5-trienyl]-1,1-dimethyl-3-(4-sulphonatobutyl)-1H-benz[i]indolium

2-[6-(acetylphenylamino)hexa-1,3,5-trienyl]-1,1-dimethyl-3-(4-sulphonatobutyl)-1H-benz[i]indolium synthesis

4synthesis methods

Product Name:2-[6-(acetylphenylamino)hexa-1,3,5-trienyl]-1,1-dimethyl-3-(4-sulphonatobutyl)-1H-benz[i]indolium
CAS Number:63450-66-8
Molecular formula:C32H34N2O4S
Molecular Weight:542.7

63149-24-6 Synthesis

1,1,2-TRIMETHYL-3-(4-SULFOBUTYL)-1H-BENZ[E]INDOLIUM HYDROXIDE, INNER SALT

63149-24-6
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N-(5-phenyliminopenta-1,3-dienyl)aniline

5608-83-3
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108-24-7
5 suppliers
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2-[6-(acetylphenylamino)hexa-1,3,5-trienyl]-1,1-dimethyl-3-(4-sulphonatobutyl)-1H-benz[i]indolium

63450-66-8
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Yield:63450-66-8 91.65%

Reaction Conditions:

for 0.166667 h;Time;

Steps:

7 Synthesis of Compound 3

Compound 1 (86.36 mg, 0.25 mmol)And compound 2 (78.32 mg, 0.275 mmol) was added to boiling acetic anhydride (500 mL) with stirring, stirred for 10 min, cooled to room temperature and filtered.The filter cake is washed with acetone and dried.Got blue and black solid,The blue-black solid was Compound 3 (124.34 mg, 91.65%).

References:

CN108264475,2018,A Location in patent:Paragraph 0035; 0045; 0053; 0054; 0055

63149-24-6 Synthesis

63149-24-6
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$26.00/250mg

108-24-7
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$14.00/250ML

1497-49-0
210 suppliers
$12.00/5g

63450-66-8
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References

63149-24-6 Synthesis

63149-24-6
99 suppliers
$26.00/250mg

1497-49-0
210 suppliers
$12.00/5g

63450-66-8
11 suppliers
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References

41532-84-7 Synthesis

41532-84-7
373 suppliers
$8.00/5g

63450-66-8
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References