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63658-16-2

(Z)-Methyl 2-(tert-butoxycarbonylaMino)but-2-enoate synthesis

2synthesis methods
56776-41-1 Synthesis
2-Butenoic acid, 2-[[(1,1-dimethylethoxy)carbonyl]amino]-, methyl ester, (2E)-

56776-41-1
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Yield:63658-16-2 90%

Reaction Conditions:

with iodine in tetrahydrofuran at 20; for 19 h;Inert atmosphere;optical yield given as %de;

References:

Kometani, Miki;Ihara, Kohki;Kimura, Rumi;Kinoshita, Hideki [Bulletin of the Chemical Society of Japan,2009,vol. 82,# 3,p. 364 - 380] Location in patent:experimental part