ChemicalBook CAS DataBase List Ethanone, 1-(2-amino-4-chlorophenyl)-2-chloro- (9CI)

Ethanone, 1-(2-amino-4-chlorophenyl)-2-chloro- (9CI) synthesis

2synthesis methods

Product Name:Ethanone, 1-(2-amino-4-chlorophenyl)-2-chloro- (9CI)
CAS Number:64605-37-4
Molecular formula:C8H7Cl2NO
Molecular Weight:204.05

1-(2'-AcetaMido-2,4'-dichlorophenyl)ethan-1-one

68095-20-5
9 suppliers
$165.00/100mg

Ethanone, 1-(2-amino-4-chlorophenyl)-2-chloro- (9CI)

64605-37-4
12 suppliers
$165.00/10mg

Yield:64605-37-4 93%

Reaction Conditions:

Stage #1: N-[5-Chloro-2-(2-chloro-acetyl)-phenyl]-acetamidewith hydrogenchloride;water in ethanol; for 1 h;Reflux;
Stage #2: with sodium hydroxide in ethanol;water; pH=Ca. 9;

References:

Cinelli, Maris A.;Morrell, Andrew E.;Dexheimer, Thomas S.;Agama, Keli;Agrawal, Surbhi;Pommier, Yves;Cushman, Mark [Bioorganic and Medicinal Chemistry,2010,vol. 18,# 15,p. 5535 - 5552] Location in patent:experimental part

107-14-2 Synthesis

107-14-2
284 suppliers
$15.00/25g

108-42-9 Synthesis

108-42-9
464 suppliers
$10.00/5g

64605-37-4
12 suppliers
$165.00/10mg

References