Carbamic acid, [(3S,5S)-5-(hydroxymethyl)-3-pyrrolidinyl]-, 1,1-dimethylethyl synthesis
- Product Name:Carbamic acid, [(3S,5S)-5-(hydroxymethyl)-3-pyrrolidinyl]-, 1,1-dimethylethyl
- CAS Number:663948-85-4
- Molecular formula:C10H20N2O3
- Molecular Weight:216.28
64187-48-0
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663948-85-4
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Yield:-
Steps:
Multi-step reaction with 6 steps
1: 99 percent / pyridine / cooling
2: 98.5 percent / NaN3 / dimethylformamide / 8 h / 70 °C
3: H2 / Raney Nickel / methanol; H2O / 1.5 h / 2068.59 Torr
4: 3.17 g / Et3N / dimethylsulfoxide / 8 h
5: 70 percent / LiBH4 / tetrahydrofuran / 3.5 h
6: H2 / Pd-C / methanol / 7 h / 3102.89 Torr
References:
Meena;Kumar, Vaijayanti A. [Bioorganic and Medicinal Chemistry,2003,vol. 11,# 16,p. 3393 - 3399]
380648-94-2
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113490-74-7
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117811-78-6
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207304-86-7
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663948-85-4
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