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6-(3-phenylprop-2-enoyl)-3,4-dihydro-2H-1,4-benzoxazin-3-one synthesis

2synthesis methods
26518-71-8 Synthesis
6-ACETYL-2H-1,4-BENZOXAZIN-3(4H)-ONE

26518-71-8
81 suppliers
$45.00/10mg

6-(3-phenylprop-2-enoyl)-3,4-dihydro-2H-1,4-benzoxazin-3-one

665021-94-3
3 suppliers
inquiry

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Yield:665021-94-3 87%

Reaction Conditions:

with sodium methylate in methanol at 50; for 24 h;

References:

Hasui, Tomoaki;Matsunaga, Nobuyuki;Ora, Taiichi;Ohyabu, Norio;Nishigaki, Nobuhiro;Imura, Yoshimi;Igata, Yumiko;Matsui, Hideki;Motoyaji, Takashi;Tanaka, Toshimasa;Habuka, Noriyuki;Sogabe, Satoshi;Ono, Midori;Siedem, Christopher S.;Tang, Tony P.;Gauthier, Cassandra;De Meese, Lisa A.;Boyd, Steven A.;Fukumoto, Shoji [Journal of Medicinal Chemistry,2011,vol. 54,# 24,p. 8616 - 8631] Location in patent:experimental part