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676542-82-8

BUPH1 , 4,7-di(9H-carbazol-9-yl)-1,10-phenanthroline synthesis

1synthesis methods
-

Yield:676542-82-8 55%

Reaction Conditions:

Stage #1: 9H-carbazolewith potassium tert-butylate in tetrahydrofuran; for 1 h;Inert atmosphere;Reflux;
Stage #2: 4,7-dichloro-1,10-phenanthroline in tetrahydrofuran; for 24 h;Inert atmosphere;Reflux;

References:

Müller, Andressa V.;Ramos, Luiz D.;Frin, Karina P. M.;De Oliveira, Kleber T.;Polo, André S. [RSC Advances,2016,vol. 6,# 52,p. 46487 - 46494]