![](/StructureFile/ChemBookStructure6/GIF/CB3717985.gif)
3-(3,5-DIMETHOXY-PHENYL)-3-OXO-PROPIONIC ACID METHYL ESTER synthesis
- Product Name:3-(3,5-DIMETHOXY-PHENYL)-3-OXO-PROPIONIC ACID METHYL ESTER
- CAS Number:677326-64-6
- Molecular formula:C12H14O5
- Molecular Weight:238.24
![Methyl acetate](/CAS/GIF/79-20-9.gif)
79-20-9
533 suppliers
$14.00/100g
![3,5-DIMETHOXYBENZOYL CHLORIDE](/CAS/GIF/17213-57-9.gif)
17213-57-9
118 suppliers
$7.00/1g
![3-(3,5-DIMETHOXY-PHENYL)-3-OXO-PROPIONIC ACID METHYL ESTER](/StructureFile/ChemBookStructure6/GIF/CB3717985.gif)
677326-64-6
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Yield:677326-64-6 88%
Reaction Conditions:
Stage #1: acetic acid methyl esterwith lithium hexamethyldisilazane in tetrahydrofuran at -78; for 0.75 h;Inert atmosphere;
Stage #2: 3,5-dimethoxybenzoyl chloride in tetrahydrofuran at -78; for 0.5 h;Inert atmosphere;
References:
Sandridge, Matthew J.;France, Stefan [Organic Letters,2016,vol. 18,# 17,p. 4218 - 4221] Location in patent:supporting information
![3',5'-Dimethoxyacetophenone](/CAS/GIF/39151-19-4.gif)
39151-19-4
190 suppliers
$17.00/250mg
![Dimethyl carbonate](/CAS/GIF/616-38-6.gif)
616-38-6
660 suppliers
$5.00/5G
![3-(3,5-DIMETHOXY-PHENYL)-3-OXO-PROPIONIC ACID METHYL ESTER](/StructureFile/ChemBookStructure6/GIF/CB3717985.gif)
677326-64-6
14 suppliers
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