(S, S)-1,2-Bis(1-naphthyl)-1,2-ethanediamine dihydrochloride synthesis

1synthesis methods

Product Name:(S, S)-1,2-Bis(1-naphthyl)-1,2-ethanediamine dihydrochloride
CAS Number:677723-26-1
Molecular formula:C22H20N2
Molecular Weight:312.41

66-77-3
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(S, S)-1,2-Bis(1-naphthyl)-1,2-ethanediamine dihydrochloride

677723-26-1
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: dimethyl sulfoxide / 20 °C / Inert atmosphere
2: hydrogenchloride; water / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

References:

Robinson, Sophia G.;Wu, Xiangyu;Jiang, Binyang;Sigman, Matthew S.;Lin, Song [Journal of the American Chemical Society,2020,vol. 142,# 43,p. 18471 - 18482]