4-(5-formylfuran-2-yl)-N-methylbenzene-1-sulfonamide synthesis

3synthesis methods

Product Name:4-(5-formylfuran-2-yl)-N-methylbenzene-1-sulfonamide
CAS Number:68502-14-7
Molecular formula:C12H11NO4S
Molecular Weight:265.29

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4-(5-formylfuran-2-yl)-N-methylbenzene-1-sulfonamide

68502-14-7
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: 40 percent / B(i-PrO)3; n-BuLi / tetrahydrofuran / 18 h / -78 - 20 °C
2: K₂CO₃ / Pd(dppf)Cl₂ / tetrahydrofuran; H₂O / 0.08 h / 120 °C / microwave irradiation

References:

Richardson, Christine M.;Nunns, Claire L.;Williamson, Douglas S.;Parratt, Martin J.;Dokurno, Pawel;Howes, Rob;Borgognoni, Jenifer;Drysdale, Martin J.;Finch, Harry;Hubbard, Roderick E.;Jackson, Philip S.;Kierstan, Peter;Lentzen, Georg;Moore, Jonathan D.;Murray, James B.;Simmonite, Heather;Surgenor, Allan E.;Torrance, Christopher J. [Bioorganic and Medicinal Chemistry Letters,2007,vol. 17,# 14,p. 3880 - 3885]

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226396-31-2 Synthesis

(4-METHYLAMINOSULPHONYL)BENZENE BORONIC ACID

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References

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References