2-azido-2-deoxy-1,3,4,6-tetraacetate β-D-Galactopyranose synthesis

5synthesis methods

Product Name:2-azido-2-deoxy-1,3,4,6-tetraacetate β-D-Galactopyranose
CAS Number:68733-19-7
Molecular formula:C14H19N3O9
Molecular Weight:373.32

14196-86-2
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108-24-7
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2-azido-2-deoxy-1,3,4,6-tetraacetate β-D-Galactopyranose

68733-19-7
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Yield:68733-19-7 96%

Reaction Conditions:

Stage #1: β-galactosylaminewith sodium azide;trifluoromethylsulfonic anhydride;potassium carbonate;copper(II) sulfate in methanol;dichloromethane;water;
Stage #2: acetic anhydridewith pyridine;dmap in methanol;dichloromethane;water;

References:

Zhou, Zhifang;Ding, Wenzhang;Li, Chen;Wu, Zhimeng [Journal of Carbohydrate Chemistry,2017,vol. 36,# 4-6,p. 205 - 219]

71141-99-6
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108-24-7
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68733-19-7
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References

108-24-7
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68733-26-6
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1,3,4,6-TETRA-O-ACETYL-2-AZIDO-2-DEOXY-ALPHA-D-GALACTOPYRANOSE

67817-30-5
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$44.79/100MG

68733-19-7
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References

68733-26-6
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108-24-7
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67817-30-5
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68733-19-7
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References

127-09-3 Synthesis

127-09-3
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2-AZIDO-2-DEOXY-D-GALACTOPYRANOSE, 3,4,6-TRIACETATE 1-NITRATE

196398-25-1
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67817-30-5
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68733-19-7
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References