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Methanaminium, N-[bis(dimethylamino)methylene]-N-methyl-, cyanide (9CI) synthesis

2synthesis methods
7677-24-9 Synthesis
Trimethylsilyl cyanide

7677-24-9
370 suppliers
$19.00/5g

Methanaminium, N-[bis(dimethylamino)methylene]-N-methyl-, methyl carbonate (1:1)

1283076-09-4
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Methanaminium, N-[bis(dimethylamino)methylene]-N-methyl-, cyanide (9CI)

68897-45-0
4 suppliers
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Yield:68897-45-0 92%

Reaction Conditions:

in acetonitrile at 0 - 20; for 1.25 h;Schlenk technique;

References:

Finger, Lars H.;Scheibe, Benjamin;Sundermeyer, J?rg [Inorganic Chemistry,2015,vol. 54,# 19,p. 9568 - 9575] Location in patent:supporting information