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2-NITRO-1-[5-NITRO-1-(PHENYLMETHYL)-1H-IMIDAZOL-4-YL] ETHANONE synthesis

6synthesis methods
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Yield:69195-97-7 68%

Reaction Conditions:

Stage #1: 5-nitro-1-(phenylmethyl)-1H-imidazole-4-carboxylic acidwith 1,1'-carbonyldiimidazole in tetrahydrofuran; for 1 h;Heating;
Stage #2: nitromethanewith potassium tert-butylate at 0 - 5;

References:

Chen, Bang-Chi;Chao, Sam T.;Sundeen, Joseph E.;Tellew, John;Ahmad, Saleem [Tetrahedron Letters,2002,vol. 43,# 9,p. 1595 - 1596]

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