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7-(2-CHLOROPHENYL)-7-OXOHEPTANENITRILE synthesis

2synthesis methods
Cycloheptene, 1-(2-chlorophenyl)-

100713-43-7
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7-(2-CHLOROPHENYL)-7-OXOHEPTANENITRILE

898767-80-1
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Yield:898767-80-1 86%

Reaction Conditions:

with 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical;trimethylsilylazide;oxygen in acetonitrile at 95; for 120 h;Schlenk technique;

References:

Wang, Teng;Jiao, Ning [Journal of the American Chemical Society,2013,vol. 135,# 32,p. 11692 - 11695] Location in patent:supporting information

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