7-Benzothiazolamine,2-methyl-(9CI) synthesis

11synthesis methods

Product Name:7-Benzothiazolamine,2-methyl-(9CI)
CAS Number:5036-87-3
Molecular formula:C8H8N2S
Molecular Weight:164.23

34564-34-6 Synthesis

Benzothiazole, 2-methyl-7-nitro- (6CI,7CI,8CI,9CI)

34564-34-6
5 suppliers
inquiry

5036-87-3
19 suppliers
inquiry

Yield:5036-87-3 1.0 g

Reaction Conditions:

with palladium on activated charcoal;hydrogen in methanol at 30; under 3800.26 Torr;

Steps:

H

[00320] Reduction of 1 .1 g of nitro compound with 0.1 1 g Pd/C in 150 ml. methanol under 5 atm of hydrogen at 30°C afforded 1.0 g of 2-methyl-1 ,3-benzothiazol-7-amine.

References:

WO2014/113492,2014,A2 Location in patent:Paragraph 00320

7439-89-6
434 suppliers
$10.00/25g

34564-34-6 Synthesis

34564-34-6
5 suppliers
inquiry

5036-87-3
19 suppliers
inquiry

References

21115-69-5
5 suppliers
inquiry

5036-87-3
19 suppliers
inquiry

References

7(4H)-Benzothiazolone, 5,6-dihydro-2-methyl-, oxime

33082-04-1
0 suppliers
inquiry

5036-87-3
19 suppliers
inquiry

References

99-09-2 Synthesis

99-09-2
9 suppliers
$14.00/1g

5036-87-3
19 suppliers
inquiry

References