ChemicalBook CAS DataBase List 7-BroMo-9,9-diMethyl-2-fluorenol

7-BroMo-9,9-diMethyl-2-fluorenol synthesis

3synthesis methods

Product Name:7-BroMo-9,9-diMethyl-2-fluorenol
CAS Number:1256619-51-8
Molecular formula:C15H13BrO
Molecular Weight:289.17

4569-45-3
212 suppliers
$7.00/5g

1256619-51-8
26 suppliers
inquiry

Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: aluminum (III) chloride / 1,2-dichloro-ethane
1.2: 20 °C
2.1: 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid / chloroform / 20 °C
3.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 20 °C
4.1: sodium hydroxide; water / ethanol / 0.17 h / 20 °C

References:

Wu, Jie;Liu, Wei;Liang, Li;Gan, Ya;Xia, Shuang;Gou, Xiaojun;Sun, Xiaohua [Tetrahedron Letters,2020,vol. 61,# 22,art. no. 151917]

5419-55-6
373 suppliers
$12.00/5g

28320-32-3 Synthesis

28320-32-3
228 suppliers
$6.00/1g

1256619-51-8
26 suppliers
inquiry

References

1-(9,9-DiMethyl-9H-fluoren-2-yl)ethanone

72322-75-9
12 suppliers
$305.00/250mg

1256619-51-8
26 suppliers
inquiry

References