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7-Methyl-azepan-2-one synthesis

6synthesis methods
7-Methyl-azepan-2-one

538369-20-9
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Yield:538369-20-9 100%

Reaction Conditions:

with Caswell No. 744A;methanesulfonic acid in 1,2-dimethoxyethane at -30 - 25; for 3 h;Inert atmosphere;

References:

Lavinda, Olga;Witt, Collin H.;Woerpel, K. A. [Angewandte Chemie - International Edition,2022,vol. 61,# 14,art. no. E202114183][Angew. Chem.,2022,vol. 134,# 14] Location in patent:supporting information