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ChemicalBook CAS DataBase List 7-Nitro-1(3H)-isobenzofuranone

7-Nitro-1(3H)-isobenzofuranone synthesis

4synthesis methods
6744-85-0 Synthesis
3-NITRO-PHTHALIC ACID 2-METHYL ESTER

6744-85-0
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: Triethylamin / tetrahydrofuran / 1 h / 0 - 2 °C
2: 65 percent / NaBH4 / tetrahydrofuran / 1 h / 0 °C

References:

Stanetty, Peter;Rodler, Inge;Krumpak, Barbara [Journal fur Praktische Chemie - Chemiker-Zeitung,1993,vol. 335,# 1,p. 17 - 22]