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18346-05-9

7-PHENYL-7H-PURINE synthesis

4synthesis methods
-

Yield:70786-03-7 64% ,18346-05-9 3%

Reaction Conditions:

with N4,N7-bis(2-hydroxyethyl)-1,10-phenanthroline-4,7-diamine;sodium L-ascorbate;potassium hydroxide;copper(I) bromide in water;N,N-dimethyl-formamide at 120; for 48 h;Inert atmosphere;Sealed tube;regioselective reaction;

References:

Larsen, Anders Foller;Ulven, Trond [Chemical Communications,2014,vol. 50,# 39,p. 4997 - 4999] Location in patent:supporting information