6-BROMO-4-CHLORO-7,7-DIMETHYL-7H-PYRANO[2,3-D]PYRIMIDINE synthesis

2synthesis methods

Product Name:6-BROMO-4-CHLORO-7,7-DIMETHYL-7H-PYRANO[2,3-D]PYRIMIDINE
CAS Number:701232-63-5
Molecular formula:C9H8BrClN2O
Molecular Weight:275.53

701232-62-4 Synthesis

6-BROMO-7,7-DIMETHYL-7H-PYRANO[2,3-D]PYRIMIDIN-4-OL

701232-62-4
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6-BROMO-4-CHLORO-7,7-DIMETHYL-7H-PYRANO[2,3-D]PYRIMIDINE

701232-63-5
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Yield:701232-63-5 99%

Reaction Conditions:

with trichlorophosphate at 100; for 1 h;

References:

Fox, Brian M.;Sugimoto, Kazuyuki;Iio, Kiyosei;Yoshida, Atsuhito;Zhang, Jian;Li, Kexue;Hao, Xiaolin;Labelle, Marc;Smith, Marie-Louise;Rubenstein, Steven M.;Ye, Guosen;McMinn, Dustin;Jackson, Simon;Choi, Rebekah;Shan, Bei;Ma, Ji;Miao, Shichang;Matsui, Takuya;Ogawa, Nobuya;Suzuki, Masahiro;Kobayashi, Akio;Ozeki, Hidekazu;Okuma, Chihiro;Ishii, Yukihito;Tomimoto, Daisuke;Furakawa, Noboru;Tanaka, Masahiro;Matsushita, Mutsuyoshi;Takahashi, Mitsuru;Inaba, Takashi;Sagawa, Shoichi;Kayser, Frank [Journal of Medicinal Chemistry,2014,vol. 57,# 8,p. 3464 - 3483] Location in patent:supporting information

31058-93-2 Synthesis

31058-93-2
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701232-63-5
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References