ChemicalBook CAS DataBase List 9-Azabicyclo[3.3.1]nonan-3-ol, 9-(phenylmethyl)-, endo-

9-Azabicyclo[3.3.1]nonan-3-ol, 9-(phenylmethyl)-, endo- synthesis

1synthesis methods

Product Name:9-Azabicyclo[3.3.1]nonan-3-ol, 9-(phenylmethyl)-, endo-
CAS Number:70243-51-5
Molecular formula:C15H21NO
Molecular Weight:231.33

2291-58-9 Synthesis

9-Azabicyclo[3.3.1]nonan-3-one, 9-(phenylmethyl)-

2291-58-9
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9-Azabicyclo[3.3.1]nonan-3-ol, 9-(phenylmethyl)-, 9-exo-

2291-60-3
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9-Azabicyclo[3.3.1]nonan-3-ol, 9-(phenylmethyl)-, endo-

70243-51-5
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Yield:40 % ee

Reaction Conditions:

with trans-RuCl₂[dppb][ammp];potassium tert-butylate;hydrogen in isopropyl alcohol at 25; under 7600.51 Torr; for 3 h;Overall yield = 93 %;Time;Concentration;Solvent;Reagent/catalyst;

Steps:

4

A reduction reaction of a 9-benzyl-9-azabicyclo[3.3.1]nonan-3-one was conducted under the conditions shown in Table 4. The results are shown in Table 4

References:

US2016/200726,2016,A1 Location in patent:Paragraph 0102

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