Bromo 2-Deoxy-2-N-phthalimido-3,4,6-tri-O-acetyl-α,β-D-glucopyranoside synthesis

7synthesis methods

Product Name:Bromo 2-Deoxy-2-N-phthalimido-3,4,6-tri-O-acetyl-α,β-D-glucopyranoside
CAS Number:70831-94-6
Molecular formula:C20H20BrNO9
Molecular Weight:498.28

4-METHOXYPHENYL 3,4,6-TRI-O-ACETYL-2-DEOXY-2-PHTHALIMIDO-BETA-D-GLUCOPYRANOSIDE

138906-41-9
37 suppliers
$39.20/1G

Bromo 2-Deoxy-2-N-phthalimido-3,4,6-tri-O-acetyl-α,β-D-glucopyranoside

70831-94-6
16 suppliers
$765.00/1g

2-Deoxy-2-phthalimido-3,4,6-tri-O-acetyl-beta-D-glucopyranosyl bromide

10028-45-2
1 suppliers
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Yield:10028-45-2 96%

Reaction Conditions:

with Acetyl bromide;boron trifluoride diethyl etherate;zinc(II) iodide in chloroform at 50; for 4 h;Yields of byproduct given. Title compound not separated from byproducts;

References:

Zhang, Zhiyuan;Magnusson, Goeran [Carbohydrate Research,1996,vol. 295,p. 41 - 55]

10022-13-6 Synthesis