1-Isoquinolinemethanamine, 1,2,3,4-tetrahydro-6,7-dimethoxy- synthesis

1synthesis methods

Product Name:1-Isoquinolinemethanamine, 1,2,3,4-tetrahydro-6,7-dimethoxy-
CAS Number:70835-34-6
Molecular formula:C12H18N2O2
Molecular Weight:222.28

41993-68-4 Synthesis

6,7-DIMETHOXY-1,2,3,4-TETRAHYDRO-ISOQUINOLINE-1-CARBOXYLIC ACID ETHYL ESTER

41993-68-4
11 suppliers
inquiry

1-Isoquinolinemethanamine, 1,2,3,4-tetrahydro-6,7-dimethoxy-

70835-34-6
0 suppliers
inquiry

Yield:-

Steps:

Multi-step reaction with 3 steps
1: ammonia / methanol / 240 h / 20 °C
2: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / Reflux
3: sodium hydroxide

References:

Kivel?, Henri;T?htinen, Petri;Martiskainen, Olli;Pihlaja, Kalevi;Lázár, László;Vigóczki, Edina;Fül?p, Ferenc [Journal of Molecular Structure,2010,vol. 983,# 1-3,p. 62 - 72]