[1]Benzothieno[2,3-d]pyrimidine-3(4H)-acetonitrile, 2-(chloromethyl)-5,6,7,8-tetrahydro-4-oxo- synthesis

1synthesis methods

Product Name:[1]Benzothieno[2,3-d]pyrimidine-3(4H)-acetonitrile, 2-(chloromethyl)-5,6,7,8-tetrahydro-4-oxo-
CAS Number:731795-75-8
Molecular formula:C13H12ClN3OS
Molecular Weight:293.77

89567-03-3 Synthesis

3-d)pyrimidin-4(1h)-one,5,6,7,8-tetrahydro-2-(chloromethyl)-(1)benzothieno(

89567-03-3
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$310.00/100mg

107-14-2 Synthesis

107-14-2
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$15.00/25g

[1]Benzothieno[2,3-d]pyrimidine-3(4H)-acetonitrile, 2-(chloromethyl)-5,6,7,8-tetrahydro-4-oxo-

731795-75-8
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Yield:731795-75-8 71%

Reaction Conditions:

with N-ethyl-N,N-diisopropylamine in N,N-dimethyl-formamide at 60 - 70;

References:

Kulik, Svetlana N.;Kobko, Alexander S.;Tolmachev, Andrey A.;Tverdokhlebov, Anton V.;Shishkin, Oleg V.;Chernega, Alexander N. [Synthesis,2007,# 10,p. 1503 - 1508]