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1H-[1,3]Dioxolo[4,5-j]pyrrolo[3,2,1-de]phenanthridine-1,2-diol, 2,4,5,7,12b,12c-hexahydro-, 1-acetate, (1S,2S,12bS,12cS)- synthesis

1synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: pyridine / methanol / 15 h / 20 - 50 °C
2: hydrogenchloride / methanol / 1 h / 55 °C

References:

Wang, Peng;Yuan, Hui-Hui;Zhang, Xue;Li, Yun-Ping;Shang, Lu-Qing;Yin, Zheng [Molecules,2014,vol. 19,# 2,p. 2469 - 2480]