Welcome to chemicalbook!
Chinese English Japanese Germany Korea
400-158-6606
Try our best to find the right business for you.
Do not miss inquiry messages Please log in to view all inquiry messages.

Welcome back!

(4-Carbamoylcyclohexylmethyl)-carbamic acid tert-butyl ester and enantiomer synthesis

3synthesis methods
-

Yield:749866-15-7 98%

Reaction Conditions:

Stage #1: trans 4-(tert-butyloxycarbonylamino)methylcyclohexanecarboxylic acidwith 1,1'-carbonyldiimidazole in tetrahydrofuran at 20; for 1 h;
Stage #2: with ammonia in tetrahydrofuran at 20; for 5 h;

References:

Li, Liantao;Mayer, Matthias;Schneider, Erich;Schreiber, Elvira;Bernhardt, Guenther;Peng, Shiqi;Buschauer, Armin [Archiv der Pharmazie,2003,vol. 336,# 12,p. 585 - 590]

(4-Carbamoylcyclohexylmethyl)-carbamic acid tert-butyl ester and enantiomer Related Search: